Category: 827320-59-2

Adding a certain compound to certain chemical reactions, such as: 827320-59-2, name is 1-butylsulfonic-3-methylimidazolium hydrogensulfate, belongs to imidazoles-derivatives compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 827320-59-2, Recommanded Product: 827320-59-2

Weigh the compound obtained in the second step1-sulfobutyl-3-methylimidazole bisulfate ionic liquid (5.06 g, 16.0 mmol)Placed in the reactor;The aqueous hydroxylamine solution 2 obtained in the first step was measured2.9 ml (32.0 mmol as hydroxylamine)Slowly added dropwise to the above ionic liquid,Low temperature (? 0 ) stirring 2h,A colorless transparent reaction liquid;The reaction solution was subjected to rotary evaporation at 70 C,A white solid product was obtained1-sulfobutyl-3-methylimidazole bisulfate ionic liquid-type hydroxylamine salt,The ionic liquid-type hydroxylamine salt was weighed and dried to weigh 4.25 g,The yield was 69.5%.

At the same time, in my other blogs, there are other synthetic methods of this type of compound, 1-butylsulfonic-3-methylimidazolium hydrogensulfate, and friends who are interested can also refer to it.

Reference:
Patent; Hebei University of Technology; Wang, Yanji; Li, Zhihui; Qi, Xudong; Zhang, Dongsheng; Xu, Yuanyuan; Yang, Quisheng; Zhao, Xinqiang; (7 pag.)CN104086487; (2016); B;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem

Adding a certain compound to certain chemical reactions, such as: 827320-59-2, name is 1-butylsulfonic-3-methylimidazolium hydrogensulfate, belongs to imidazoles-derivatives compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 827320-59-2, Formula: C8H16N2O7S2

Synthesis of 1-Sulfobutyl-3-methylimidazole Sulfate Ionic LiquidHydroxylamine Salts: Weigh the 1-sulfobutyl-3-methylimidazolium bisulfate ionic liquidobtained in the second step 5.06 (16.0 mmol) was placed in the reactor. 22.9 ml (32.0mmol of hydroxylamine) was added dropwise to the above ionic liquid in the first step,and the mixture was stirred at a low temperature (? 0 C) for 2 hours, The reactionsolution was evaporated at 70 C to give a white solid product 1-sulfobutyl-3-methylimidazole bisulfate ionic liquid type hydroxylamine salt. After the ionic liquidtype hydroxylamine salt was dried, Weighing 4.25 g, the yield was 69.5%.

If you are interested in these compounds, you can also browse my other articles.Thank you for taking the time to read this article. I hope you enjoyed it.

Reference:
Patent; Hebei University of Technology; WANG, YANJI; LI, ZHIHUI; ZHANG, DONGSHENG; QI, XUDONG; XU, YUANYUAN; YANG, QIUSHENG; ZHAO, XINQIANG; (7 pag.)CN104086474; (2016); B;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem