Category: 79917-88-7

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 79917-88-7, name is 1,3-Dimethyl-1H-imidazol-3-ium chloride, This compound has unique chemical properties. The synthetic route is as follows., COA of Formula: C5H9ClN2

Take a 100 mL three-necked flask,1,3-dimethylimidazole was added thereto successively under nitrogen protection(1.33 g0 · 01 mol), acetone (100 mL, 1.71 mol) and then 30percent methanol sodium methoxide solution (1.8 g, 0.01 mol) was added to control the reaction temperature at 15 ° C. After 4 h of reaction, the reaction solution was filtered and the filtrate was charged into a 250 mL autoclave.

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 79917-88-7.

Reference:
Patent; Guangdong Laifoshi Pharmaceutical Co., Ltd.; Zhou Zhangtao; Xu Junye; Fei Anjie; Tan Chuanwen; Huang Zhining; Xiao Shihua; Yan Yannan; (5 pag.)CN106892807; (2017); A;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem

Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 79917-88-7, name is 1,3-Dimethyl-1H-imidazol-3-ium chloride, A new synthetic method of this compound is introduced below., Quality Control of 1,3-Dimethyl-1H-imidazol-3-ium chloride

(1) Take 10g mass purity1,3-dimethyl-imidazolium chloride 25mL of distilled water was added to dissolve the solid, was added 55mL of 30percent concentration of hydrofluoric acid, stirred and heated to 50oC in the original closed;(2) reaction of starting material at least sufficient 3h, then heated to 100oC, excess hydrogen fluoride was evaporated and the product gas of hydrogen chloride gas, tail gas absorption using calcium oxide, not dehydrated to give 1,3-dimethyl-imidazol-fluorinated ionic liquids;(3) not to dehydrated 1,3-dimethylimidazolidinone fluorinated ionic liquid was diluted with distilled water was added, the volume is not dehydrated 1,3-dimethyl-fluorinated ionic liquid with distilled water, is less than 1:50, was added to the AgNO3 solution was diluted, if precipitation production, continue to add 20mL hydrofluoric acid, repeating (1) and (2) step until no precipitate was produced, purified non-dehydrated 1,3-dimethylimidazolidinone fluoride ionic liquids;(4) dewatering the non-purified non-dehydrated 1,3-dimethylimidazolidinone fluoride at 120oC ionic liquid was dried under high vacuum at least 48h, in addition to the depth of water, in addition to hydrogen fluoride, to give a viscous liquid of viscosity liquid detection, viscous liquid was added to distilled water, distilled water with viscous liquid volume ratio of less than 1:50, sealed and heated to 30oC, with hydrogen detector dilution residual amount of hydrogen fluoride, if the reading is greater than> 0.1ppm, continue to 120oC and dried under high vacuum in addition to fluorideHydrogen until the concentration of hydrogen fluoride test <0.1ppm; detecting if the hydrogen fluoride concentration <0.1ppm, the resultant liquid is 1,3-dimethylimidazolidinone fluorinated ionic liquids, weighing 8.52g. The synthetic route of 79917-88-7 has been constantly updated, and we look forward to future research findings. Reference:
Patent; Beijing University; Li, Zhongning; Zhong, Xiongwei; Xiong, Ting; Hu, Xianwei; Xu, Junli; Wang, Zhaowen; Gao, Bingliang; Yu, Jiangyu; (27 pag.)CN103992275; (2016); B;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 79917-88-7, name is 1,3-Dimethyl-1H-imidazol-3-ium chloride, This compound has unique chemical properties. The synthetic route is as follows., Application In Synthesis of 1,3-Dimethyl-1H-imidazol-3-ium chloride

1) 33.81 g of 1,3-dimethylimidazolium chloride (purity 99percent) and 7.6 g of NH4F (purity 98percent) were respectively taken, and the two solids were directly placed in an Erlenmeyer flask and ultrasonically shaken in a water bath at 50 ¡ãC. 8h, the solid will undergo a metathesis reaction to produce a white precipitate, which is allowed to stand, precipitate and settle, and the upper layer is a liquid phase with suspended particles to obtain a layered mixture after standing;2) pumping the layered phase at a low pressure three times to obtain a filtrate and a filter residue;3) The liquid phase obtained by filtration is vacuum-screwed at 60 ¡ã C to obtain a pale yellow clear liquid;4) Dry the light yellow clear solution at 70 ¡ã C for 24 h to obtain a light yellow viscous liquid, which is a 1,3-dimethylfluoroimidazole product, label L4, using a small glass bottle and taking two drops of product for Raman Spectral detection test to check whether the product contains NH4+, compare the spectral results of the sample with the standard Raman spectrum of NH4+, if the comparison shows the presence of NH4+The Raman vibration band continues to dry at 100 ¡ã C under high vacuum until the Raman vibration band without NH4+ is detected. If the Raman vibration band without NH4+ is detected, the obtained 1,3-dimethylfluorinated imidazolium ionic liquid is weighed. 23.19g.

According to the analysis of related databases, 79917-88-7, the application of this compound in the production field has become more and more popular.

Reference:
Patent; Northeastern University (disambiguation); Hu Xianwei; Niu Chunbo; Shi Zhongning; Gao Bingliang; Yu Jiangyu; Wang Zhaowen; (11 pag.)CN108586347; (2018); A;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem