Analyzing the synthesis route of 1-Butyl-3-methylimidazolium methanesulfonate

The synthetic route of 342789-81-5 has been constantly updated, and we look forward to future research findings.

Reference of 342789-81-5,Some common heterocyclic compound, 342789-81-5, name is 1-Butyl-3-methylimidazolium methanesulfonate, molecular formula is C9H18N2O3S, traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.

5.3-1-Butyl-3-methylimidazolium N-trifluoro-sulfonamidate [BMI.(CF3SO2)2N]A mixture formed by 1,3-dimethyl imidazolium methanesulfonate (BMI.CH3SO3) (4.26 g; 18.2 mmol), lithium N-trifluoro sulfonimidate (5.47 g; 19.1 mmol) and water (10.0 mL) was stirred at room temperature for 45 minutes. The resulting mixture, made up by two phases, was extracted with dichloromethane (3×15 mL). The combined organic extract was washed with water (1×20 mL) and dried with anhydrous sodium carbonate. The solvent was evaporated under vacuum and heated (80 C.), which produced the desired ionic liquid BMI.(CF3SO2)2N (7.33 g. 96% yield).

The synthetic route of 342789-81-5 has been constantly updated, and we look forward to future research findings.

Reference:
Patent; PETROLEO BRASILEIRO S.A. – PETROBRAS; US2008/45723; (2008); A1;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem

Brief introduction of 342789-81-5

These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route 1-Butyl-3-methylimidazolium methanesulfonate, its application will become more common.

Reference of 342789-81-5,Some common heterocyclic compound, 342789-81-5, name is 1-Butyl-3-methylimidazolium methanesulfonate, molecular formula is C9H18N2O3S, traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.

5.2-1-butyl-3-methylimidazolium hexafluorophosphate (BMI.BF4)A mixture formed by 1,3-dimethyl imidazolium methanesulfonate (BMI.CH3SO3) (5.80 g; 24.6 mmol), sodium hexafluorophosphate (5.00 g; 29.8 mmol) and water (5.0 mL) was stirred at room temperature for 30 minutes. The resulting mixture, made up by two phases, was extracted with dichloromethane (3¡Á10 mL). The combined organic extract was washed with water (2¡Á20 mL) and dried with anhydrous sodium carbonate. The solvent was evaporated under vacuum and heated (80 C.), which produced the desired ionic liquid BMI.PF6 (6.64 g; 95% yield).

These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route 1-Butyl-3-methylimidazolium methanesulfonate, its application will become more common.

Reference:
Patent; PETROLEO BRASILEIRO S.A. – PETROBRAS; US2008/45723; (2008); A1;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem

The important role of 1-Butyl-3-methylimidazolium methanesulfonate

The synthetic route of 1-Butyl-3-methylimidazolium methanesulfonate has been constantly updated, and we look forward to future research findings.

Application of 342789-81-5, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 342789-81-5, name is 1-Butyl-3-methylimidazolium methanesulfonate belongs to imidazoles-derivatives compound, it is a common compound, a new synthetic route is introduced below.

5.1-1-butyl-3-methylimidazolium tetrafluoroborate (BMI.BF4)A mixture formed by 1,3-dimethyl imidazolium methanesulfonate (BMI.CH3SO3) (10.6 g; 45.0 mmol), sodium tetrafluoroborate (6.00 g; 54.5 mmol) and water (5.4 mL) was stirred at room temperature for 30 minutes. The resulting mixture, made up of two phases, was extracted with dichloromethane (3¡Á15 mL). The combined organic extract was dried with anhydrous sodium carbonate and the solvent was evaporated under vacuum and heated (80 C.), which produced the desired BMI.BF4 ionic liquid. (9.35 g; 92% yield).

The synthetic route of 1-Butyl-3-methylimidazolium methanesulfonate has been constantly updated, and we look forward to future research findings.

Reference:
Patent; PETROLEO BRASILEIRO S.A. – PETROBRAS; US2008/45723; (2008); A1;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem