Extracurricular laboratory: Synthetic route of 145022-45-3

These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route 145022-45-3, its application will become more common.

Some common heterocyclic compound, 145022-45-3, name is 1-Ethyl-3-methylimidazolium Methanesulfonate, molecular formula is C7H14N2O3S, traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route. 145022-45-3

For the Emim3[PMo12O40] (from this point forward Emim-Mo)synthesis [30], appropriate quantities of prepared H3PMo12O40(0.9 g) and 1-ethyl-3-methylimidazolium methanesulfonate (Alfa Aesar) were dissolved in distilled water (20 mL) separately. When mixed, a precipitate was formed, then filtered and dried at room temperature. Another two hybrids were analogously prepared by using 1-butyl-3-methylimidazolium methanesulfonate (Sigma Aldrich) to produce the Bmim3[PMo12O40] (Bmim-Mo) and 1-hexyl-3-methylimidazolium chloride (Alfa Aesar) for Hexmim3[PMo12O40] (Hexmim-Mo). All the hybrids were used asprepared and their structures are presented in Fig. 1

These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route 145022-45-3, its application will become more common.

Reference:
Article; Megias-Sayago; Carrasco; Ivanova; Montilla; Galindo; Odriozola; Catalysis Today; vol. 278; (2016); p. 82 – 90;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem