17334-08-6, name is (1-Methyl-1H-imidazol-2-yl)methanol, belongs to imidazoles-derivatives compound, is considered to be a conventional heterocyclic compound, which is widely used in drug synthesis. The chemical synthesis route is as follows. Safety of (1-Methyl-1H-imidazol-2-yl)methanol
2-Chloromethyl-1-methyl-imidazolhydrochloride The 2-chloromethyl-1-methyl-imidazolhydrochloride is produced according to the description above. 20 ml thionylchloride is added to a suspension of 5.61 g 1-methylimidazolyl-1-methanol in 5 ml dry benzene. Two phases are built. Stir vigorously for half an hour. Then the combined solvents are rotated off and a bright brown product remains. 1H-NMR (CDCl3; 270 MHz): 7.75 (d; 1H); 7.68 (d; 1H); 5.16 (s; 2H); 3.86 (s, 3H); 3.42 (s; 3H). 13C-NMR: 141.5; 124.7; 119.4; 34.2; 31.7 ppm.
The synthetic route of 17334-08-6 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Unilever Home & Personal Care USA, division of Conopco, Inc.; US6646122; (2003); B1;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem