Reference of 21252-69-7,Some common heterocyclic compound, 21252-69-7, name is 1-Octyl-1H-imidazole, molecular formula is C11H20N2, traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
Silver(I)-N-octylimidazole complexes were alsosynthesized using a previously reported method with a minor modification. Typically, N-octylimidazole (2 mol equiv.) was added to a solution of AgNO3 (1 mol equiv.) in ethanol (15 mE) and the reaction mixture was stirred at room temperature for 24 h. The reaction mixture was filtered and evaporation of the solvent mixture gave a brown oil or cream solid. The brown oil was re-dissolved in dichloromethane and extracted three times with watet The organic phase was dried on anhydrous sodium sulfate and the solvent was removed under reduced pressure. Other silver(I)-N-alkylimidazole complexes were synthesized in the same manner. The solid complexes were further purified by recrystallization by dissolving in dichloromethane and precipitated with hexane.
The synthetic route of 21252-69-7 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Kleyi, Phumelele; Maity, Arjun; Ray, Suprakas Sinha; (16 pag.)US2018/255777; (2018); A1;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem