9/3/2021 News Brief introduction of 583-39-1

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Adding a certain compound to certain chemical reactions, such as: 583-39-1, name is 2-Mercaptobenzimidazole, belongs to imidazoles-derivatives compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 583-39-1, Safety of 2-Mercaptobenzimidazole

A mixture of 0.1 g of benzimidazole-2-thione, 0.374 g of benzyl acetate 1, and 5 mL of methanol was kept at room temperature for 20 days. The precipitate was filtered off, washed with methanol, and dried in air. Yield 0.21 g (54%), mp 243-245C (mp 244-245C [13]). 1H NMR spectrum (CDCl3), delta, ppm: 1.42 s (36H, CMe3), 5.18 s (2H,OH ), 5.52 s (4H, CH2N), 7.12-7.25 m (4H, ArH), 7.40 s (4H, ArH).

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Reference:
Article; Gataullina; Mogilevtseva; Nugumanova; Bukharov; Tagasheva; Deberdeev, R. Ya.; Russian Journal of General Chemistry; vol. 87; 9; (2017); p. 1919 – 1923; Zh. Obshch. Khim.; vol. 87; 9; (2017); p. -1435 – -1439,5;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem