Synthetic Route of 33529-02-1, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 33529-02-1, name is 1-Decyl-1H-imidazole, This compound has unique chemical properties. The synthetic route is as follows.
1-Decylimidazole was synthesized according to previous literature. 1-Decylimidazole (5.49 g, 26.3 mmol) and 3-bromopropene (3.1 g, 26.3 mmol) were added to a 100 mL round-bottom flask containing 30 mL ethanol with condenser. The reaction mixture was stirred for 24 h. Solvent was then removed under reduced pressure. The crude product was washed three times with ether and dried in a vacuum oven at 50 C for 24 h to give the 1-allyl-3-decylimidazolium bromide (ADIm). 1-Allyl-3-decylimidazolium bromide: This compound was obtained in 97% as a yellow viscous oil. 1H NMR (DMSO-d6, 400 MHz): delta 9.30 (s, 1H, -N-CH-N-), 7.87 (s, 1H, -N-CH-CH-N-), 7.78 (s, 1H, -N-CH-CH-N-), 6.07 (m, 1H, -CH=CH2), 5.32 (dd, 2H, =CH2), 4.87 (d, 2H, -CH2-CH=CH2), 4.19 (t, 2H, -N-CH2-), 1.79 (m, 2H, -CH2-CH2-), 1.24 (broad, 14H, -CH2-CH3), 0.85 (t, 3H, -CH3).
The chemical industry reduces the impact on the environment during synthesis 1-Decyl-1H-imidazole. I believe this compound will play a more active role in future production and life.
Reference:
Article; Zhou, Chuan; Li, Yi-He; Jiang, Zhen-Hua; Ahn, Kwang-Duk; Hu, Tian-Jiao; Wang, Qing-Hua; Wang, Chun-Hua; Chinese Chemical Letters; vol. 27; 5; (2016); p. 685 – 688;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem