Reference of 1072-63-5, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 1072-63-5, name is 1-Vinyl-1H-imidazole belongs to imidazoles-derivatives compound, it is a common compound, a new synthetic route is introduced below.
Comprising the steps of: 0.840 g of alpha-mercaptomethyltrimethoxysilane prepared in Example 6 and 1.176 g of 1-Vinylimidazole were placed in a round bottom flask wrapped in aluminum box paper. Then, 8 mL of tetrahydrofuran was added, and after mixing uniformly, 0.076 g of benzoin dimethyl ether was added, the mixture was uniformly stirred, the aluminum box paper was removed, and irradiated at room temperature for 30 minutes under a UV lamp having a power of 20 W and a wavelength of 365 nm. After the completion of the reaction, the solvent was distilled off under reduced pressure, and the degree of vacuum was 5 to 6 mmHg, which was precipitated three times in n-hexane, and dried under vacuum at 40 C to a constant weight to obtain alpha-(1-ethylimidazolyl)mercaptomethyltrimethoxysilane, purity 96%, yield 96%. The infrared spectrum of the product alpha-(1-ethylimidazolyl)mercaptomethyltrimethoxysilane obtained in this example is shown in Fig. 19, and the nuclear magnetic resonance spectrum is shown in Fig. 20. 19 and 20, the product obtained in this example was alpha-(1-ethylimidazolyl)mercaptomethyltrimethoxysilane
The synthetic route of 1-Vinyl-1H-imidazole has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Shandong University; Bei Yiling; Gao Yanhong; Zhu Qingzeng; Feng Shengyu; (24 pag.)CN109053794; (2018); A;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem