Synthetic Route of 27231-33-0, The chemical industry reduces the impact on the environment during synthesis 27231-33-0, name is 4-Methyl-1H-benzo[d]imidazole-2(3H)-thione, I believe this compound will play a more active role in future production and life.
EXAMPLE 7 2-[[(4-Methyl-1H-benzimidazol-2-yl)thio]methyl]benzenamine The title compound was prepared by the method of Example 1 using 3.52 g of 2-mercapto-4-methylbenzimidazole instead of 2-mercaptobenzimidazole and 3.52 g of 2-(chloromethyl) aniline hydrochloride instead of 2-(chloromethyl)-N,N-dimethylaniline. Recrystallization from diethyl ether gave 1.23 g of the title compound: m.p. 125-127 C. Anal. Calc’d. for C15 H15 N3 S: C, 66.89; H, 5.61; N,15.60; S, 11.90. Found: C, 66.76; H, 5.62; N, 15.41; S, 11.87.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 4-Methyl-1H-benzo[d]imidazole-2(3H)-thione, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; G.D. Searle & Co.; US5945425; (1999); A;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem