Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 33529-02-1, name is 1-Decyl-1H-imidazole, A new synthetic method of this compound is introduced below., HPLC of Formula: C13H24N2
(2) Add 50 mL of ethanol to a four-neck round bottom flask.Further added 19.35 g (0.05 mol) of N,N-dimethyl(1-bromopropyl)decyl ammonium bromide, 10.42 g (0.05 mol)N-decylimidazole and1 g of tetrabutylammonium bromide,The mixture was heated to 70 C with stirring, and the reaction was stirred for 36 hours, and then ethanol was distilled off under reduced pressure.The solid was washed three times with chloroform.The filter cake was vacuum dried at 60 C for 5 hours to obtain a crude product;The crude product is recrystallized three times in acetone to obtain the product.1-(N,N-dimethylammonium alkylammonium) propyl-3-hydrazinium imidazolium dibromide,The yield was 85.8%.
The synthetic route of 33529-02-1 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Zhengzhou University of Light Industry; Yang Xuzhao; Wang Jun; Li Yakun; Ping Dan; Zhang Yingying; Wu Shide; (8 pag.)CN109970657; (2019); A;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem