Extracurricular laboratory: Synthetic route of

Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 914306-50-6, name is 1-(2,6-Diisopropylphenyl)-2-phenyl-1H-imidazole, A new synthetic method of this compound is introduced below., SDS of cas: 914306-50-6

A 50 mL Schlenk tube flask was charged with N-(2,6-diisopropyl phenyl)-2- phenylimidazole (7.60 g, 25 mmol), tris(acetylacetonate)iridium(III) (2.45 g, 5.0 mmol) and tridecane (1 mL). The reaction mixture was stirred under a nitrogen atmosphere and heated at EPO 240 C for 48 hours. After cooling, the solidified mixture was washed first with absolute ethanol followed by hexane. The residue was further purified by a silica gel column to give fac-mc6 (1.5 g). The product was further purified by vacuum sublimation. 1H and MS results confirmed the desired compound. lambdamax of emission = 476, 504 nm (CH2Cl2 solution at room temperature), CIE = (0.22, 0.43).

The synthetic route of 914306-50-6 has been constantly updated, and we look forward to future research findings.

Reference:
Patent; UNIVERSAL DISPLAY CORPORATION; WO2008/54584; (2008); A1;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem