Synthetic Route of 872-82-2, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 872-82-2, name is 2-(1H-Imidazol-5-yl)ethanol belongs to imidazoles-derivatives compound, it is a common compound, a new synthetic route is introduced below.
0.291 g (1 mmol) of cobalt(II) nitrate hexahydrate was dissolvedin 5 mL of methanol. In a separate flask 0.224 g (2 mmol) 4(5)-(bhydroxyethyl)imidazole was dissolved in 5 mL of methanol. Bothsolutions were mixed and refluxed for 60 min. The resulting solutionwas left to evaporate in room temperature. After severalmonths reddish crystals of 1 were formed in the initially obtainedpink oil. Anal. calcd. for CoC10H20N6O10 (442.03 g/mol): C 27.10; H4.55; N 18.96, found: C 27.11; H 4.26; N 19.78. M.p. 355 K. FT-IR(solid): t = 3224 (vs), 2929 (s), 1655 (w), 1591 (w), 1575 (w),1501 (w), 1474 (w), 1331 (vs), 1269 (s), 1188 (m), 1105 (m),1090 (w), 1064 (w), 1044 (w), 1022 (s), 964 (w), 946 (w), 857(w), 821 (m), 771 (w), 657 (w), 637 (w), 621 (m), 501 (w) cm1.Vis spectra of aqueous solutions are presented in Supplementarycontent (Fig. 1S).
The synthetic route of 2-(1H-Imidazol-5-yl)ethanol has been constantly updated, and we look forward to future research findings.