Electric Literature of 1615-14-1, The chemical industry reduces the impact on the environment during synthesis 1615-14-1, name is 2-(1H-Imidazol-1-yl)ethanol, I believe this compound will play a more active role in future production and life.
The mixture of 1-(2-hydroxyethyl)imidazole (2 g, 0.017 mol)and 1-chlorododecane (4.2 g, 0.02 mol) was stirred at 140 C for24 h under an argon atmosphere. The obtained semi-solid productwas purified bywashing with hexane-ethyl acetate mixture (4:1 (v/v), 3 30 ml). Residual solvents were removed in vacuum10 mbar at 70e80 C for 12 h. The ionic liquid has melting point of28e29 C.1H NR (400 Hz, DMSO-D6): d 0.85 (t, 3H, CH3), 1.25 (m,18H, H3(CH2)9),1.79 (m, 2H, NCH2CH2), 3.38 (br s,1H, OH), 3.72 (m,2H, NCH2CH2OH), 4.16e4.23 (m, 4, NCH2), 7.78 (br s, 1H, C4eH),7.81 (br s, 1H, C5eH), 9.27 (s, 1H, C2eH).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 2-(1H-Imidazol-1-yl)ethanol, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Trush, Maria M.; Semenyuta, Ivan V.; Vdovenko, Sergey I.; Rogalsky, Sergiy P.; Lobko, Evgeniya O.; Metelytsia, Larisa O.; Journal of Molecular Structure; vol. 1137; (2017); p. 692 – 699;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem