Some common heterocyclic compound, 1615-14-1, name is 2-(1H-Imidazol-1-yl)ethanol, molecular formula is C5H8N2O, traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route. Product Details of 1615-14-1
In a reaction vessel, 1.12 g of N-hydroxyethyl imidazole and 50 mL of tetrahydrofuran are added, and 20 drops are added under stirring.1.55g per minuteIsocyanoethyl methacrylate,The reaction was carried out at 45 C. for 12 hours to complete the reaction of the isocyanate groups. Then, the reaction temperature was adjusted to 65 C., 2.49 g of bromdecane was added, and the reaction was carried out for 72 hours to produce a product, which was then purified to obtain an A2B12F monomer.
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route 1615-14-1, its application will become more common.
Reference:
Patent; South China University of Technology; He Jingwei; Liu Fang; Zhu Wenbin; (9 pag.)CN107162981; (2017); A;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem