Electric Literature of 570-22-9, In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 570-22-9 as follows.
A mixture of Zn(NO3)2ยท6H2O (0.0291g, 0.1mmol), Hcptpy (0.0277g, 0.05mmol), and H3idc (0.0126g, 0.1mmol) in distilled water (10mL) that adjusted the pH value to 4.5 with 0.5molL-1 NaOH aqueous solution was placed in a Teflon-lined tainless steel vessel (25mL), heated to 180 for 72h and then cooled to room temperature at a rate of 5/h. The yellow sheet crystalline products of 2 were obtained, washed with distilled water (5mL), and dried in air to give 0.0321g (yield 61.8% based on Zn). Anal. Calc. for C49H31N8Zn2O11 (%): C, 56.67; H, 3.00; N, 10.79. Found: C, 56.52; H, 3.08; N, 10.32%. IR(KBr, cm-1): 3133(s), 1596(m), 1548(m), 1401(vs), 1251(w), 1132(w), 870(w), 829(m), 784(m), 707(m), 634(w), 517(w).
According to the analysis of related databases, 570-22-9, the application of this compound in the production field has become more and more popular.
Reference:
Article; Yuan, Fei; Wang, Ting-Ting; Hu, Huai-Ming; Li, Chuan-Ti; Zhou, Chun-Sheng; Wang, Xiaofang; Xue, Ganglin; Journal of Solid State Chemistry; vol. 251; (2017); p. 79 – 89;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem