Share a compound : 1792-40-1

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 2-Methyl-5-nitro-1H-benzo[d]imidazole, other downstream synthetic routes, hurry up and to see.

Related Products of 1792-40-1, The chemical industry reduces the impact on the environment during synthesis 1792-40-1, name is 2-Methyl-5-nitro-1H-benzo[d]imidazole, I believe this compound will play a more active role in future production and life.

In 100mL round bottom flask, 2-methyl-5-nitrobenzimidazole (0. 46g, 0. 0026mol), potassium carbonate (0 · 72g, 0 · 0052mol) and the amount of acetonitrile, temperature control The reaction was stirred 50 C 0 · 5h, cooled to room temperature, was added II-2 (1. 00g, 0. 0026mol) was heated to 80 C and stirring continued, until thin layer chromatography the reaction was completed track, and then by concentration, extraction, column chromatographic separation, recrystallization, and dried to give square 0. 49g Compound 1-30, yield 33.4%.

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 2-Methyl-5-nitro-1H-benzo[d]imidazole, other downstream synthetic routes, hurry up and to see.

Reference:
Patent; Southwest University; Zhou, Chenghe; Zhang, Ling; (39 pag.)CN104086534; (2016); B;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem