In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 1072-62-4 as follows. SDS of cas: 1072-62-4
EXAMPLE 2 2-Ethyl-4,5-dihydroxymethylimidazole The procedure described in Example 1 is followed, except that 96 g (1 mole) of 2-ethylimidazole are used instead of 2-methylimidazole. The 155 g of crude product obtained in this procedure are stirred with 52 g of methanol for 30 minutes at 50 C. and at 10 C. with cooling. The mixture is filtered, the product is washed with twice 150 ml of acetone and dried in a drying oven, and 117.5 g of 2-ethyl-4,5-dihydroxymethylimidazole of melting point 173.35-174.0 C. are obtained. This corresponds to a yield of 75.4%. The purity of this sample is 99.8% according to HPLC. Elemental analysis: Mass spectrum: M+ 156. 1 H-NMR spectrum (solvent DDMSO) 1.15 (t, 1p) 2.55 (q, 2p) 4.4 (s, 4p).
According to the analysis of related databases, 1072-62-4, the application of this compound in the production field has become more and more popular.
Reference:
Patent; BASF Aktiengesellschaft; US4658035; (1987); A;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem