Application of 65039-05-6, A common heterocyclic compound, 65039-05-6, name is 1-Butyl-3-methylimidazolium iodide, molecular formula is C8H15IN2, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
General procedure: The preparation of BiOI microspheres was carried out bysolvothermal synthesis. All reagents used were of analytical grade (AR) and used as received without additional purification. 1 mmolof bismuth nitrate pentahydrate [Bi(NO3)3.5H2O] (Sigma-Aldrich,99.0%) was dissolved in ethylene glycol (10 mL, Merck 99.5%) andpoured in a solution of 10 mL of ethylene glycol containing 1 mmolof KI (99.0% Merck). The mixture was stirred at room temperaturefor 30 min and then transferred to a 23 mL Teflon autoclave reactor.The autoclave was heated at 126 C (at autogenous pressure) for18 h andfinally cooled to room temperature. Thefinal productswere separated by vacuumfiltration and extensively washed usingdistilled water and absolute ethanol (Merck, 99.5% v/v). Thematerial obtained was dried at 60 C for 24 h. The same procedurewas used to synthesize BiOI using ionic liquid 1-butyl-3-methylimidazolium iodide ([bmim]I) as an iodide source.
The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.
Reference:
Article; Mera, Adriana C.; Contreras, David; Escalona, Nestor; Mansilla, Hector D.; Journal of Photochemistry and Photobiology A: Chemistry; vol. 318; (2016); p. 71 – 76;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem