Adding a certain compound to certain chemical reactions, such as: 60-56-0, name is 1-Methyl-1H-imidazole-2(3H)-thione, belongs to imidazoles-derivatives compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 60-56-0, Application In Synthesis of 1-Methyl-1H-imidazole-2(3H)-thione
Aroyl chloride (1 mmol) was added to a stirred solution of ammonium thiocyanate (1 mmol) in 10 mL MeCN. The mixture was stirred at room temperature (r.t.) for 30 min. Then, 2-mercapto-1-methylimidazole (1 mmol) was added and the reaction mixture was stirred for 2 h at r.t. The solvent was removed under reduced pressure and the resulting precipitate was collected and washed with 10 mL ofcold diethyl ether to afford the pure title compounds.
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