Reference of 33529-02-1, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 33529-02-1, name is 1-Decyl-1H-imidazole belongs to imidazoles-derivatives compound, it is a common compound, a new synthetic route is introduced below.
General procedure: Under an atmosphere of nitrogen, the alpha,omega-bis(methanesulfonyloxy)alkane (0.36 mmol, 1 equiv) was mixed with the appropriate 1-alkylimidazole(5 equiv) and the mixture was heated at 80-90 C for 1 h;acetone (20 mL) was then added and the mixture was stirred at refluxtemperature overnight, concentrated, and dried under high vacuum.The resulting golden oil was dissolved in methanol, the solution wasconcentrated, and the residual oil was washed with diethyl ether(10 mL). This dissolution/concentration/washing procedure was repeatedtwo more times. The solid material was dried under high vacuumto give the product.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 1-Decyl-1H-imidazole, other downstream synthetic routes, hurry up and to see.