Electric Literature of 45676-04-8, The chemical industry reduces the impact on the environment during synthesis 45676-04-8, name is 1-tert-Butylimidazole, I believe this compound will play a more active role in future production and life.
F) 1,1′-Di-tert-butyl-3,3′-methylenediimidazolium diiodide 13 0.008 mol of diiodomethane (2.143 g; 0.64 ml) and 5 ml of tetrahydrofuran are added to 0.016 mol of tertbutylimidazole 2 (2.000 g) in an ACE pressure tube. The reaction mixture is stirred at 80 C. for 3 hours. The precipitated solid is washed repeatedly with a little tetrahydrofuran. The white solid 13 is obtained. Empirical formula: C15H26N4I2 M=516.198 g/mol Yield: 1.444 g (35.0% of theory) Melting point: decomposition at >249 C. 1H (ppm, d6-DMSO, 300.13 MHz): delta=9.55 (s, 2H, NCN); 8.17 (s, 2H, NCCHN); 8.06 (s, 2H, NCHCN); 6.54 (s, 2H, NC2N); 1.61 (s, 18H, C3 group)
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 1-tert-Butylimidazole, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; BASF SE; TECHNISCHE UNIVERSITAET DRESDEN; US2009/326237; (2009); A1;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem