Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 195053-92-0, name is 2-(1-Trityl-1H-imidazol-4-yl)ethanamine, This compound has unique chemical properties. The synthetic route is as follows., Recommanded Product: 195053-92-0
To synthesize Limz1 2-(1-trityl-1H-imidazol-4-yl-)ethyl amine (1.00 g, 2.83 mmol), trimethylacetaldehyde(0.62 mL, 5.66 mmol, 2 eq.) and sodium sulfate (10.1 g,70.7 mmol, 25 eq.) were dissolved in dry toluene (15 mL).The mixture was stirred at room temperature for at least3 h. The residue was filtered off and washed twice withdry toluene (2 ¡Á 3 mL). The solvent was removed untila colorless solid precipitated. After 24 h the solid was filtered,washed with acetonitrile and dried in vacuum toafford Limz1 (728 mg, 1.23 mmol, 61 %) as a white powder.Anal. calcd. for C29H31N3: C (82.62 %); H (7.41 %); N(9.97 %); found C (82.56 %); H (7.50 %); N (9.90 %). 1HNMR(CDCl3, 400 MHz): delta = 7.46 (t, J = 1.2 Hz, 1H, imidazoleH-2), 7.37-7.27 (m, 9H, Ar-H), 1.15-7.10 (m, 6H,Ar-H), 6.56 (s, 1H, imidazole H-5), 3.64 (t, J = 7.0 Hz,2H, -CH2-CH2-N-), 2.82 (t, J = 7.0 Hz, 2H, -CH2-CH2-N-), 0.97 (s, 9H, -C(CH3)3) ppm. 13C-NMR (CDCl3,100 MHz): delta = 172.5 (CH, 1C, -N=CH-C(CH3)3), 142.8(C, 3C, phenyl C-1), 139.5 (C, 1C, imidazole C-4), 138.4 (CH, 1C, imidazole C-2), 129.9 (CH, 6C, phenyl C-3, C-5),128.1 (CH, 6C, phenyl C-2, C-6), 128.0 (CH, 3C, phenylC-4), 118.7 (CH, 1C, imidazole C-5), 75.2 (C, 1C, -N-C-(C6H6)3), 60.6 (CH2, 1C, -CH2-CH2-N=), 36.0 (C, 1C,=CH-C(CH3)3), 30.2 (CH2, 1C, -CH2-CH2-N=), 27.1 (C,3C, =CH-C(CH3)3) ppm.
According to the analysis of related databases, 195053-92-0, the application of this compound in the production field has become more and more popular.
Reference:
Article; Wendt, Franziska; Naether, Christian; Tuczek, Felix; Journal of Biological Inorganic Chemistry; vol. 21; 5-6; (2016); p. 777 – 792;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem