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Synthesis, crystal structure, and spectral properties of a novel Co(II) complex containing imidazole derivative
A novel imidazole derivative with functional group and pi-conjugated system, 1-[trans-4-(4-diethylaminostyryl)phenyl]imidazole (abbreviated as L), and its Co-II complex (CoCl2L4)(2) (Co2C168H184N24Cl4, M-r = 2799.05) have been synthesized and the crystal structure of the latter was determined by X-ray diffraction. The crystal is of triclinic, space group P (1) over bar with a 8.823(3), b = 18.799(7), c = 23.065(9) angstrom, alpha = 77.349(6), beta = 83.128(7), gamma = 80.942(3)degrees, V 3671.5(12) angstrom(3), Z = 1, D-c = 1.266 g/cm(3), mu = 0.361 mm(-1), F(000) = 1482, the final R = 0.0587 and wR = 0.1284 for 6562 observed reflections with I > 2 sigma(I). In the molecular, structure of (CoCl2L4)(2), there are two crystallographically unique units. The Co-II atoms are six-coordinated by four N atoms from four imidazole ligands (L) and two Cl atoms to form a distorted octahedral geometry. The optical properties of complex (CoCl2L4)(2) have been experimentally studied.
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