Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 10040-96-7, name is 1-(4-Bromophenyl)imidazole, This compound has unique chemical properties. The synthetic route is as follows., Product Details of 10040-96-7
Pd(PPh3)4 (112 mg, 96.7 mumol) was added to a mixture of 6 (600 mg, 0.967 mmol) and 1-(4-bromophenyl)-1H-imidazole (863 mg, 3.87 mmol) in aqueous Na2CO3 (2 M, 2.0 mL, 4.0 mmol) and anhydrous THF (18.0 mL), and the solution was stirred at room temperature for 15 min. The resulting two-phase system was refluxed under stirring overnight, and was then allowed to cool to room temperature. To this was added water (50 mL), and the mixture was extracted with CHCl3 (100 mL¡Á3). The organic layer was washed with water (50 mL), dried over anhydrous MgSO4, and filtered. After the solvent was removed by evaporation, the residue was subjected to SEC fractionation to obtain 2 (516 mg, 79%) as a bluish white solid. Mp: 251.8-252.0 C. IR (KBr, cm-1): 1523, 1305, 1273, 1139, 1114, 1055, 989. 1H NMR (500 MHz, CDCl3): delta 7.89 (s, 2H, ArH), 7.65 (d, J=8.6 Hz, 4H, PhH), 7.42 (d, J=8.6 Hz, 4H, PhH), 7.32 (s, 2H, ArH), 7.25 (s, 2H, ArH), 2.01 (s, 6H, CH3). 13C NMR (125 MHz, CDCl3): delta 142.1, 140.9, 136.9, 135.6, 132.7, 130.9, 127.1, 126.2, 123.1, 122.0, 118.2, 14.8. MS (ESI+): m/z=653 [M+H]+. Anal. Calcd for C33H22F6N4S2: C, 60.73; H, 3.40; N, 8.58. Found: C, 60.74; H, 3.48; N, 8.45.
According to the analysis of related databases, 10040-96-7, the application of this compound in the production field has become more and more popular.
Reference:
Article; Iida, Hiroki; Umebayashi, Naofumi; Yashima, Eiji; Tetrahedron; vol. 69; 52; (2013); p. 11064 – 11069;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem