Application of 1072-63-5, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 1072-63-5 name is 1-Vinyl-1H-imidazole, This compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
In a round bottom flask, bromoethane (4.07 g, 0.367 mol) was added dropwise to 1-vinylimidazole (2.10 g, 0.213 mol),The reaction was refluxed at 40 C for 16 hours.The yellow-white solid obtained by filtration was washed several times with ethyl acetate and dried in a vacuum oven.The ionic liquid monomer ViEtlmBr was obtained.Yield: 3.27 g (76%).
At the same time, in my other blogs, there are other synthetic methods of this type of compound, 1-Vinyl-1H-imidazole, and friends who are interested can also refer to it.
Reference:
Patent; Liaoning University; Xia Lixin; Wang Kaili; Jiang Yi; (16 pag.)CN108677211; (2019); B;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem