Introduction of a new synthetic route about 827320-59-2

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Adding a certain compound to certain chemical reactions, such as: 827320-59-2, name is 1-butylsulfonic-3-methylimidazolium hydrogensulfate, belongs to imidazoles-derivatives compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 827320-59-2, Formula: C8H16N2O7S2

Synthesis of 1-Sulfobutyl-3-methylimidazole Sulfate Ionic LiquidHydroxylamine Salts: Weigh the 1-sulfobutyl-3-methylimidazolium bisulfate ionic liquidobtained in the second step 5.06 (16.0 mmol) was placed in the reactor. 22.9 ml (32.0mmol of hydroxylamine) was added dropwise to the above ionic liquid in the first step,and the mixture was stirred at a low temperature (? 0 C) for 2 hours, The reactionsolution was evaporated at 70 C to give a white solid product 1-sulfobutyl-3-methylimidazole bisulfate ionic liquid type hydroxylamine salt. After the ionic liquidtype hydroxylamine salt was dried, Weighing 4.25 g, the yield was 69.5%.

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Reference:
Patent; Hebei University of Technology; WANG, YANJI; LI, ZHIHUI; ZHANG, DONGSHENG; QI, XUDONG; XU, YUANYUAN; YANG, QIUSHENG; ZHAO, XINQIANG; (7 pag.)CN104086474; (2016); B;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem