Adding a certain compound to certain chemical reactions, such as: 3304-70-9, name is Dimethyl 4,5-imidazoledicarboxylate, belongs to imidazoles-derivatives compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 3304-70-9, Recommanded Product: Dimethyl 4,5-imidazoledicarboxylate
Dimethyl 1H-imidazole-4,5-dicarboxylate (8 g, 43 mmol) was added with about 50 to 100 ml of ammonia solution. The mixture was stirred at 10 to 120 C. for 2 to 24 hours. A large amount of white solid was precipitated. After filtration, the filter cake was washed with 50 ml of water and then washed with 50 ml of ethanol, and dried at 40 C. in an oven to obtain a product. 1HNMR (DMSO, 500 MHz): delta 10.437 (1H,s), delta 9.043 (2H,s), delta 7.769 (1H,s), delta 7.681 (2H, s)
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Reference:
Patent; GUANGZHOU INSIGHTER BIOTECHNOLOGY CO.,LTD.; PENG, Xianfeng; QIN, Zonghua; (15 pag.)US2018/370921; (2018); A1;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem