Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 760212-58-6, name is 1-(4-Bromophenyl)-2-phenyl-1H-benzo[d]imidazole, This compound has unique chemical properties. The synthetic route is as follows., Recommanded Product: 1-(4-Bromophenyl)-2-phenyl-1H-benzo[d]imidazole
500 ml three-neck bottle,Equipped with mechanical mixing and distillation unit,5.0 g (0.0091 mol) of the compound of the formula M-206 was added,3.49 g (0.0101 mol) of 4-(2-phenyl-1H-benzo[d]imidazol-1-yl)bromobenzene,40 ml of toluene,40 ml of ethanol,25 ml of water,2.51 g (0.0182 mol) of potassium carbonate,0.05 g (0.0000455 mol) of tetrakistriphenylphosphine palladium was added under nitrogen protection.After the addition, slowly warmed to 70 C,Reaction for 8 hours.Cool down, add water,The organic layer is washed,Dry over anhydrous sodium sulfate,Decolorization on silica gel column,The eluent is concentrated to dryness.The crude product P-2 was obtained.The above crude P-2 product was recrystallized from a mixed solvent of toluene and ethyl acetate to obtain 5.01 g of a product P-2.The yield was 71.3%.
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 760212-58-6.
Reference:
Patent; Fuyang Xinyihua Materials Technology Co., Ltd.; Wang Zhanqi; Li Zhiqiang; Guo Linlin; (37 pag.)CN108218788; (2018); A;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem