Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 583-39-1, name is 2-Mercaptobenzimidazole, A new synthetic method of this compound is introduced below., 583-39-1
General procedure: To an orange suspension of [Pd2(kappa2:C, N-mazb)2(mu-Cl)2] (0.025g, 0.040mmol) in dichloromethane (5mL), N-methylimidazolidine-2-thione (0.012g, 0.080mmol) was added in presence of Et3N base (0.5mL). The color of the reaction mixture became red brown and was stirred for 5-6h. The solution was filtered and methanol (5mL) was added and was left to evaporate slowly. The red brown crystals of compound 7 were obtained after a period of 4-5d.
The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.
Reference:
Article; Sandhu, Amanpreet K.; Lobana, Tarlok S.; Sran, Balkaran S.; Hundal, Geeta; Jasinski, Jerry P.; Journal of Organometallic Chemistry; vol. 861; (2018); p. 112 – 124;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem